Technology Process of C26H35NO5
There total 5 articles about C26H35NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 15h;
DOI:10.3987/COM-10-S(E)76
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / diethyl ether / 0.5 h / -78 °C
2: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 15 h / 0 - 20 °C
With
boron trifluoride diethyl etherate; sodium hydride;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
2: Williamson etherification;
DOI:10.3987/COM-10-S(E)76
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 4.5 h / 0 - 20 °C
2: boron trifluoride diethyl etherate / diethyl ether / 0.5 h / -78 °C
3: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 15 h / 0 - 20 °C
With
boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
3: Williamson etherification;
DOI:10.3987/COM-10-S(E)76