2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

Base Information

Chemical Name:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside
CAS No.:1001082-63-8
Molecular Formula:C₃₀H₃₈O₈Si
Molecular Weight:554.712
Hs Code.:

Synonyms:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

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Chemical Property of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

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Technology Process of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

There total 1 articles about 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1001082-62-7
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-mannopyranoside

: 1001082-63-8
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo701531x

Reference yield: 82.0%

: 1001082-63-8
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1001082-64-9
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Further stages.;
DOI:10.1021/jo701531x