2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Base Information

Chemical Name:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside
CAS No.:1001082-64-9
Molecular Formula:C₃₁H₄₀O₇Si
Molecular Weight:552.74
Hs Code.:

Synonyms:2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

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Chemical Property of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

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Technology Process of 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

There total 1 articles about 2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1001082-63-8
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1001082-64-9
2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-3-deoxy-3-methylene-α-D-arabino-hexopyranoside

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

2'-(allyloxycarbonyl)benzyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-α-D-arabino-hexopyranoside-3-uloside; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Further stages.;
DOI:10.1021/jo701531x