4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine

Base Information

• Chemical Name: 4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine
• CAS No.: 33006-91-6
• Molecular Formula: C₁₁H₁₀ClN₅
• Molecular Weight: 247.687
• Hs Code.: 2933399090
• European Community (EC) Number: 251-334-0
• DSSTox Substance ID: DTXSID601318521
• Nikkaji Number: J208.226H
• Mol file: 33006-91-6.mol

Synonyms:33006-91-6;4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine;4-((5-Chloropyridin-2-yl)diazenyl)benzene-1,3-diamine;4-[(5-chloropyridin-2-yl)diazenyl]benzene-1,3-diamine;EINECS 251-334-0;4-(5-Chloro-2-pyridylazo)benzene-1,3-diamine;4-(5-Chloro-2-pyridylazo)-m-phenylenediamine;4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine [for Colorimetric Analysis of Co, Cd];1,3-Benzenediamine, 4-((5-chloro-2-pyridinyl)azo)-;1,3-Benzenediamine, 4-[(5-chloro-2-pyridinyl)azo]-;5-Cl-PADAB;C11H10ClN5;SCHEMBL12805490;DTXSID601318521;MFCD00059781;AKOS024341560;AS-66953;FT-0639073;4-(5-Chloro-2-pyridylazo)-1,3-benzenediamine;4-(5-chloro-2-pyridylazo)-1,3-diaminobenzene;T70784;4-[(5-chloro-2-pyridyl)azo]-1,3-diaminobenzene;A821561;(E)-4-((5-chloropyridin-2-yl)diazenyl)benzene-1,3-diamine;4-[(E)-(5-Chloro-2-pyridinyl)diazenyl]-1,3-benzenediamine #;4-[(1E)-2-(5-chloropyridin-2-yl)diazen-1-yl]benzene-1,3-diamine

Chemical Property of 4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine

Chemical Property:

• Vapor Pressure: 1.14E-09mmHg at 25°C
• Boiling Point: 487.9°Cat760mmHg
• PKA: 2.29±0.10(Predicted)
• Flash Point: 248.9°C
• PSA: 89.65000
• Density: 1.45g/cm³
• LogP: 4.47720
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 247.0624730
• Heavy Atom Count: 17
• Complexity: 273

Purity/Quality:

97% ^*data from raw suppliers

4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine [for Colorimetric Analysis of Co, Cd] >99.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1N)N)N=NC2=NC=C(C=C2)Cl

Technology Process of 4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine

There total 1 articles about 4-(5-Chloro-2-pyridylazo)-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.8%

5-chloro-2-pyridylamine (1072-98-6) + m-phenylenediamine dihydrochloride (541-69-5,13652-74-9) + isopentyl nitrite (110-46-3) → 4-(5-chloro-2-pyridylazo)-1,3-phenylenediamine (33006-91-6)

Guidance literature:

5-chloro-2-pyridylamine; With sodium amide; In ethanol; at 0 ℃; for 2h; Reflux;

isopentyl nitrite; In ethanol; at 65 - 70 ℃;

m-phenylenediamine dihydrochloride; Further stages;

upstream raw materials:

5-chloro-2-pyridylamine

m-phenylenediamine dihydrochloride

isopentyl nitrite

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