1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

Base Information

Chemical Name:1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide
CAS No.:1426852-99-4
Molecular Formula:C₁₇H₂₀F₃N₃O
Molecular Weight:339.361
Hs Code.:

Synonyms:1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

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Chemical Property of 1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

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Technology Process of 1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

There total 2 articles about 1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1426852-95-0
3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

: 407-25-0
trifluoroacetic anhydride

: 1426852-99-4
1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

Guidance literature:: 3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate; trifluoroacetic anhydride; In tetrahydrofuran; at 0 - 25 ℃; for 3h; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/om400078f

Reference yield:

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 1426852-99-4
1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 16 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 3 h / 0 - 25 °C / Inert atmosphere

2.2: 0.17 h / 20 °C / Inert atmosphere

In tetrahydrofuran; acetonitrile;
DOI:10.1021/om400078f