3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

Base Information

Chemical Name:3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate
CAS No.:1426852-95-0
Molecular Formula:C₆H₃N₂O₅*C₁₅H₂₂N₃
Molecular Weight:427.46
Hs Code.:

Synonyms:3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

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Chemical Property of 3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

Chemical Property:

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Technology Process of 3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

There total 1 articles about 3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 17508-17-7
O-(2,4-dinitrophenyl)hydroxylamine

: 1426852-95-0
3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

Guidance literature:: In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/om400078f

Reference yield: 76.0%

: 1426852-95-0
3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

: 407-25-0
trifluoroacetic anhydride

: 1426852-99-4
1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide

Guidance literature:: 3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate; trifluoroacetic anhydride; In tetrahydrofuran; at 0 - 25 ℃; for 3h; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/om400078f

Reference yield:

: 1426852-95-0
3-amino-1-(2,6-diisopropylphenyl)-1H-imidazolium 2,4-dinitrophenolate

: [Ag₂(1-(2,6-diisopropylphenyl)-3-trifluoroacetylimino-1H-imidazolium ylide(-1H))₂]

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / 0 - 25 °C / Inert atmosphere

1.2: 0.17 h / 20 °C / Inert atmosphere

2.1: chloroform / 48 h / 20 °C / Inert atmosphere; Darkness

In tetrahydrofuran; chloroform;
DOI:10.1021/om400078f