2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose
CAS No.:150852-15-6
Molecular Formula:C₂₁H₂₅NO₁₀S
Molecular Weight:483.496
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Suppliers and Price of 2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

There total 6 articles about 2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 19879-84-6
tetraacetyl thioglucose

: 698-16-8
benzohydroximoyl chloride

: 150852-15-6
2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; at 20 ℃; for 2h; stereospecific reaction; Inert atmosphere;
DOI:10.1016/j.bmc.2013.07.049

Reference yield:

: 932-90-1,622-31-1,140461-24-1,140461-25-2,622-32-2
syn-benzaldehyde oxime

: 150852-15-6
2,3,4,6-tetra-O-acetyl-1-S-(Z)-benzhydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; N-chlorosuccinimide / CH₂Cl₂ / 2 h / 20 °C

2: triethylamine / diethyl ether; CH₂Cl₂ / 2 h / 20 °C

With pyridine; N-chloro-succinimide; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1002/jlcr.1407