2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane

Base Information

• Chemical Name: 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane
• CAS No.: 97095-57-3
• Molecular Formula: C₂₃H₁₇F₁₆O₃P
• Molecular Weight: 676.334

Synonyms:2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane

Chemical Property of 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane

Chemical Property:

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Technology Process of 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane

There total 4 articles about 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ⁵-[1,4,2]dioxaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanol (67-56-1) + 2-chloro-3,5-bis(1,1,2,2,3,3,4,4-octafluorobutyl)-2,2-diphenyl-1,4,2-dioxaphospholane (97108-41-3) → 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ5-[1,4,2]dioxaphospholane (97095-57-3)

Guidance literature:

With triethylamine; In diethyl ether; for 1h;

Reference yield:

2,2,3,3,4,4,5,5-octafluorovaleraldehyde (2648-47-7) → 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ5-[1,4,2]dioxaphospholane (97095-57-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / 1 h

2: 100 percent / triethylamine / diethyl ether / 1 h

With triethylamine; In diethyl ether;

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) → 2-Methoxy-3,5-bis-(1,1,2,2,3,3,4,4-octafluoro-butyl)-2,2-diphenyl-2λ5-[1,4,2]dioxaphospholane (97095-57-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / 1 h

2: 100 percent / triethylamine / diethyl ether / 1 h

With triethylamine; In diethyl ether;

upstream raw materials:

methanol

2-chloro-3,5-bis(1,1,2,2,3,3,4,4-octafluorobutyl)-2,2-diphenyl-1,4,2-dioxaphospholane

2,2,3,3,4,4,5,5-octafluorovaleraldehyde

chloro-diphenylphosphine

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