(R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate

Base Information

• Chemical Name: (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate
• CAS No.: 105660-54-6
• Molecular Formula: C₈H₁₁N*C₉H₁₁NS₂
• Molecular Weight: 318.507
• Mol file: 105660-54-6.mol

Synonyms:(R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate

Chemical Property of (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate

There total 1 articles about (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

carbon disulfide (75-15-0,12122-00-8) + (R)-1-phenyl-ethyl-amine (3886-69-9) → (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate (105660-54-6)

Guidance literature:

In various solvent(s); at 5 ℃;

DOI:10.1021/ja00236a030

Reference yield: 50.0%

2-buten-4-olide (497-23-4) + (R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate (105660-54-6) → 4,4'-disulfanediylbis(dihydrofuran-2-one) (192121-58-7) + C8H10O4S + (4RS)-4-{[(R)-N-α-methylbenzylamino](thiocarbonyl)thio}-4,5-dihydro-2(3H)-furanone

Guidance literature:

With acetic acid; In chloroform; at 20 ℃; for 72h;

DOI:10.1002/ejoc.200300693

Reference yield:

(R)-N-(1-phenylethyl)ammonium (R)-N-(1-phenylethyl)dithiocarbamate (105660-54-6) → (R)-3-(1-phenylethyl)-Δ4-1,3-thiazoline-2-thione (96393-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. ethanol / 5 - 20 °C / add of DMF

2: 0.01N HCl in EtOH / 0.25 h / Heating

With hydrogenchloride; In ethanol;

DOI:10.1021/ja00236a030

upstream raw materials:

carbon disulfide

(R)-1-phenyl-ethyl-amine

Downstream raw materials:

4,4'-disulfanediylbis(dihydrofuran-2-one)

(R)-3-(1-phenylethyl)-Δ⁴-1,3-thiazoline-2-thione