C₂₃H₂₁F₂N₅O₄S

Base Information

Chemical Name:C₂₃H₂₁F₂N₅O₄S
CAS No.:1415731-00-8
Molecular Formula:C₂₃H₂₁F₂N₅O₄S
Molecular Weight:501.514
Hs Code.:

C<sub>23</sub>H<sub>21</sub>F<sub>2</sub>N<sub>5</sub>O<sub>4</sub>S

Synonyms:C₂₃H₂₁F₂N₅O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₁F₂N₅O₄S

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Technology Process of C₂₃H₂₁F₂N₅O₄S

There total 4 articles about C₂₃H₂₁F₂N₅O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1415730-99-2
8-(3-phenyl[1,2,4]oxadiazol-5-yl)-1-oxa-2,8-diazaspiro[4.5]-dec-2-ene-3-carboxylic acid (2,5-difluoro-4-methylsulfanylphenyl)amide

: 1415731-00-8
C₂₃H₂₁F₂N₅O₄S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jm301549a

Reference yield:

: 112279-60-4
4-bromo-2,5-difluoroaniline

: 1415731-00-8
C₂₃H₂₁F₂N₅O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide; sodium iodide; N,N-dimethylethylenediamine / 1,4-dioxane / 3 h / 140 °C / Inert atmosphere

2.1: zinc; nickel dibromide; [2,2]bipyridinyl / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; HATU / 0.75 h / 20 °C

3.2: 3 h / 20 °C

3.3: 2 h

4.1: N-ethyl-N,N-diisopropylamine; 1-methyl-pyrrolidin-2-one / 0.25 h / 160 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

With 1-methyl-pyrrolidin-2-one; [2,2]bipyridinyl; copper(l) iodide; N,N-dimethylethylenediamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; sodium iodide; nickel dibromide; zinc; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301549a

Reference yield:

: 155906-13-1
2,5-difluoro-4-iodophenylamine

: 1415731-00-8
C₂₃H₂₁F₂N₅O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc; nickel dibromide; [2,2]bipyridinyl / N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; HATU / 0.75 h / 20 °C

2.2: 3 h / 20 °C

2.3: 2 h

3.1: N-ethyl-N,N-diisopropylamine; 1-methyl-pyrrolidin-2-one / 0.25 h / 160 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

With 1-methyl-pyrrolidin-2-one; [2,2]bipyridinyl; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; nickel dibromide; zinc; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301549a