(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

Base Information

Chemical Name:(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate
CAS No.:1408287-01-3
Molecular Formula:C₂₇H₃₀N₂O₃
Molecular Weight:430.547
Hs Code.:

Synonyms:(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

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Chemical Property of (S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

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Technology Process of (S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

There total 1 articles about (S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1408287-03-5
(S)-tert-butyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-ylcarbamate

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1408287-01-3
(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

Guidance literature:: (S)-tert-butyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-ylcarbamate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide; With sodium carbonate; In 1,4-dioxane; at 20 ℃; for 19h;
DOI:10.1021/ol302852q

Reference yield:

: 35661-60-0
Fmoc-Leu-OH

: 35737-10-1
N-Fmoc-β-alanine

: 1408287-01-3
(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

: 94744-50-0
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-α-aminoisobutyric acid

: (S)-methyl 1-butylpyrrolidine-2-carboxylate

: 1408287-00-2
C₅₃H₉₇N₁₁O₁₁

Guidance literature:: (S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 22h; 2-chlorotrityl-functionalized aminomethylpolystyrene resin Inert atmosphere;

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; 2-chlorotrityl-functionalized aminomethylpolystyrene resin

Fmoc-Leu-OH; N-Fmoc-β-alanine; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-α-aminoisobutyric acid; (S)-methyl 1-butylpyrrolidine-2-carboxylate; Reagent/catalyst;
DOI:10.1021/ol302852q

Reference yield:

: 35661-60-0
Fmoc-Leu-OH

: 35737-10-1
N-Fmoc-β-alanine

: 1408286-91-8
(2S,4S,6R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-6-hydroxy-4-methyl-8-oxodecanoic acid

: 1408287-01-3
(S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate

: 94744-50-0
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-α-aminoisobutyric acid

: (S)-methyl 1-butylpyrrolidine-2-carboxylate

: 889128-40-9
culicinin D

Guidance literature:: (S)-(9H-fluoren-9-yl)methyl 1-[benzyl(2-hydroxyethyl)amino]propan-2-yl carbamate; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 22h; 2-chlorotrityl-functionalized aminomethylpolystyrene resin Inert atmosphere;

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; 2-chlorotrityl-functionalized aminomethylpolystyrene resin

Fmoc-Leu-OH; N-Fmoc-β-alanine; (2S,4S,6R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-6-hydroxy-4-methyl-8-oxodecanoic acid; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-α-aminoisobutyric acid; (S)-methyl 1-butylpyrrolidine-2-carboxylate;
DOI:10.1021/ol302852q