5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

Base Information

Chemical Name:5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl
CAS No.:1098755-73-7
Molecular Formula:C₂₈H₃₀O₆
Molecular Weight:462.543
Hs Code.:

Synonyms:5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

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Technology Process of 5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

There total 1 articles about 5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1098755-72-6
5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1098755-73-7
5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃;

5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde; In tetrahydrofuran; hexane; at -78 - 0 ℃;
DOI:10.1021/jo802370v

Reference yield: 93.0%

: 1098755-73-7
5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

: 1098755-74-8
3-(benzyloxy)-1,2,6-trimethoxy-5-(methoxymethoxy)phenanthrene

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 40 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo802370v