5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

Base Information

Chemical Name:5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde
CAS No.:1098755-72-6
Molecular Formula:C₂₆H₂₆O₈
Molecular Weight:466.488
Hs Code.:

Synonyms:5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

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Technology Process of 5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

There total 1 articles about 5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 909766-98-9
4-benzyloxy-6-iodo-2,3-dimethoxybenzaldehyde

: 1098755-71-5
4-methoxy-3-(methoxymethoxy)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

: 1098755-72-6
5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In dimethyl sulfoxide; at 70 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jo802370v

Reference yield: 71.0%

: 1098755-72-6
5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1098755-73-7
5-(benzyloxy)-3,3',4-trimethoxy-2'-(methoxymethoxy)-2,6'-divinylbiphenyl

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃;

5-(benzyloxy)-3,4,5'-trimethoxy-6'-(methoxymethoxy)biphenyl-2,2'-dicarbaldehyde; In tetrahydrofuran; hexane; at -78 - 0 ℃;
DOI:10.1021/jo802370v