1-(Bromo(1-naphthyl)methyl)naphthalene

Base Information

Chemical Name:1-(Bromo(1-naphthyl)methyl)naphthalene
CAS No.:5467-20-9
Molecular Formula:C21H15 Br
Molecular Weight:347.254
Hs Code.:2903999090
NSC Number:28081
DSSTox Substance ID:DTXSID10969957
Nikkaji Number:J3.656.556J
Wikidata:Q82953033
ChEMBL ID:CHEMBL512832
Mol file:5467-20-9.mol

Synonyms:1-(bromo(1-naphthyl)methyl)naphthalene;5467-20-9;NSC28081;NSC-28081;1,1'-(Bromomethylene)dinaphthalene;CHEMBL512832;dinaphthylbromomethane;NCIStruc1_001175;NCIStruc2_001236;SCHEMBL11444158;DTXSID10969957;NCI28081;BDBM50262189;CCG-36823;NCGC00013347;NCGC00013347-02;NCGC00096464-01;NCI60_002284

Suppliers and Price of 1-(Bromo(1-naphthyl)methyl)naphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(Bromo(1-naphthyl)methyl)naphthalene

Chemical Property:

Boiling Point:484.4°Cat760mmHg
Flash Point:239.3°C
PSA：0.00000
Density:1.383g/cm³
LogP:6.47730
XLogP3:6.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:346.03571
Heavy Atom Count:22
Complexity:331

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC=C2C(C3=CC=CC4=CC=CC=C43)Br

Technology Process of 1-(Bromo(1-naphthyl)methyl)naphthalene

There total 7 articles about 1-(Bromo(1-naphthyl)methyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 62784-66-1
bis(1-naphthyl)methanol

: 5467-20-9
1-(bromo(1-naphthyl)methyl)naphthalene

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1055/s-0033-1338564

Reference yield:

: 90-11-9
1-Bromonaphthalene

: 5467-20-9
1-(bromo(1-naphthyl)methyl)naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 2.15 h / 20 °C

1.2: 2 h / 20 °C

2.1: phosphorus tribromide / dichloromethane / 0 - 20 °C

With iodine; phosphorus tribromide; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.7b00246