cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid

Base Information

• Chemical Name: cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid
• CAS No.: 1113007-59-2
• Molecular Formula: C₁₉H₁₈N₂O₃*ClH
• Molecular Weight: 358.824

Synonyms:cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid

Chemical Property of cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid

Chemical Property:

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Technology Process of cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid

There total 1 articles about cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,3S)-1-(3-hydroxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid (869304-05-2) + methanol (67-56-1) → cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (1113007-59-2)

Guidance literature:

With thionyl chloride; at 20 ℃;

DOI:10.1016/j.tetlet.2008.11.008

Reference yield: 87.0%

cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (1113007-59-2) + 1H-imidazole-1-carbodithioic acid methyl ester (74734-11-5) + N-butylamine (109-73-9,85404-21-3) → (5R,11aS)-2-butyl-5-(3-hydroxyphenyl)-3-thioxo-6H-1,2,3,5,11,11a-hexahydro-imidazo[1,5-b]-β-carbolin-1-one

Guidance literature:

With triethylamine; In methanol; diastereoselective reaction; Reflux;

DOI:10.1016/j.tetlet.2008.11.008

Reference yield: 85.0%

cis-1-(3-hydroxy)phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (1113007-59-2) + 3-trifluoromethylaniline (98-16-8) + 1H-imidazole-1-carbodithioic acid methyl ester (74734-11-5) → C26H18F3N3O2S (1113007-45-6)

Guidance literature:

With triethylamine; In methanol; diastereoselective reaction; Reflux;

DOI:10.1016/j.tetlet.2008.11.008

upstream raw materials:

(1S,3S)-1-(3-hydroxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid

methanol

Downstream raw materials:

C₂₆H₂₇N₃O₄S

C₂₆H₁₈F₃N₃O₂S

C₂₅H₂₅N₃O₂S

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