20-dihydro-20-O-phenyl-2'-O-acetyltylosin

Base Information

Chemical Name:20-dihydro-20-O-phenyl-2'-O-acetyltylosin
CAS No.:91661-68-6
Molecular Formula:C₅₄H₈₅NO₁₈
Molecular Weight:1036.26
Hs Code.:

Synonyms:20-dihydro-20-O-phenyl-2'-O-acetyltylosin

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Chemical Property of 20-dihydro-20-O-phenyl-2'-O-acetyltylosin

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Technology Process of 20-dihydro-20-O-phenyl-2'-O-acetyltylosin

There total 3 articles about 20-dihydro-20-O-phenyl-2'-O-acetyltylosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1401-69-0
tylosin

: 91661-68-6
20-dihydro-20-O-phenyl-2'-O-acetyltylosin

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / sodium borohydride / propan-2-ol; H₂O / 0.5 h

2: 52 percent / triphenylphosphine, diethyl azodicarboxylate / toluene; CH₂Cl₂; tetrahydrofuran / 0.5 h / Ambient temperature

3: acetone / 16 h / Ambient temperature

With sodium tetrahydroborate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; acetone; toluene;
DOI:10.1021/jm00403a025

Reference yield:

: 1404-48-4
20-dihydrotylosin

: 91661-68-6
20-dihydro-20-O-phenyl-2'-O-acetyltylosin

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / triphenylphosphine, diethyl azodicarboxylate / toluene; CH₂Cl₂; tetrahydrofuran / 0.5 h / Ambient temperature

2: acetone / 16 h / Ambient temperature

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; acetone; toluene;
DOI:10.1021/jm00403a025