20-dihydro-20-O-phenyltylosin

Base Information

Chemical Name:20-dihydro-20-O-phenyltylosin
CAS No.:91661-59-5
Molecular Formula:C₅₂H₈₃NO₁₇
Molecular Weight:994.228
Hs Code.:

Synonyms:20-dihydro-20-O-phenyltylosin

Suppliers and Price of 20-dihydro-20-O-phenyltylosin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 20-dihydro-20-O-phenyltylosin

Chemical Property:

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Technology Process of 20-dihydro-20-O-phenyltylosin

There total 2 articles about 20-dihydro-20-O-phenyltylosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1404-48-4
20-dihydrotylosin

: 108-95-2,27073-41-2
phenol

: 91661-59-5
20-dihydro-20-O-phenyltylosin

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene; for 0.5h; Ambient temperature;
DOI:10.1021/jm00403a025

Reference yield:

: 1401-69-0
tylosin

: 91661-59-5
20-dihydro-20-O-phenyltylosin

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / sodium borohydride / propan-2-ol; H₂O / 0.5 h

2: 52 percent / triphenylphosphine, diethyl azodicarboxylate / toluene; CH₂Cl₂; tetrahydrofuran / 0.5 h / Ambient temperature

With sodium tetrahydroborate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; toluene;
DOI:10.1021/jm00403a025