N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

Base Information

Chemical Name:N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine
CAS No.:80186-06-7
Molecular Formula:C₄₅H₄₈N₆O₁₂
Molecular Weight:864.909
Hs Code.:

N<sup>6</sup>-benzoyl-3'-O-<N-(benzyloxycarbonyl)-L-phenylalanyl>-5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

Synonyms:N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

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Technology Process of N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

There total 2 articles about N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1161-13-3
N-Cbz-L-Phe

: 80186-04-5
N⁶-benzoyl-5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

: 80186-06-7
N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

Guidance literature:: With pyridine; mesitylenesulfonyl tetrazolide; for 2h;
DOI:10.1021/jo00343a007

Reference yield:

: 123-76-2
levulinic acid

: 80186-06-7
N⁶-benzoyl-3'-O--5'-O-levulinyl-2'-O-(4-methoxytetrahydropyran-4-yl)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / 1,2-dimethylimidazole, 2,6-lutidine, DCC / dioxane; dimethylformamide / 4 h / Ambient temperature

2: 84 percent / pyridine, mesitylenesulfonyl tetrazolide (MST) / 2 h

With pyridine; 2,6-dimethylpyridine; 1,2-dimethyl-1H-imidazole; mesitylenesulfonyl tetrazolide; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jo00343a007