3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

Base Information

Chemical Name:3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide
CAS No.:1453354-73-8
Molecular Formula:C₁₉H₁₅ClN₂O₃
Molecular Weight:354.793
Hs Code.:

Synonyms:3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

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Chemical Property of 3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

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Technology Process of 3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

There total 1 articles about 3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67829-05-4
1-(3-chlorophenyl)-2-hydroxyethanone

: 5341-58-2
3-hydroxy-2-naphthohydrazide

: 1453354-73-8
3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

Guidance literature:: In methanol; for 2h; Reflux;
DOI:10.1016/j.ica.2013.04.036

Reference yield: 79.0%

: 1453354-73-8
3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

: 2273-51-0
diphenyltin(IV) oxide

: {[1-(5-chloro-2-oxidophenyl)ethylidene]-3-hydroxy-2-naphthohydrazidato}diphenyltin(IV)

Guidance literature:: In toluene; Dean-Stark; Reflux;
DOI:10.1016/j.ica.2013.04.036

Reference yield: 78.0%

: 19135-40-1
di(para-chlorobenzyl)tin(IV) dichloride

: 1453354-73-8
3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide

: {[1-(5-chloro-2-oxidophenyl)ethylidene]-3-hydroxy-2-naphthohydrazidato}di(p-chlorobenzyl)tin(IV)

Guidance literature:: 3-hydroxy-N'-[(1E)-1-(2-hydroxy-5-chlorophenyl)ethylidene]-2-naphthohydrazide; With triethylamine; In ethanol; for 2h; Reflux;

di(para-chlorobenzyl)tin(IV) dichloride; In ethanol; for 2h; Reflux;
DOI:10.1016/j.ica.2013.04.036