2,6-mansyl chloride

Base Information

• Chemical Name: 2,6-mansyl chloride
• CAS No.: 18392-55-7
• Molecular Formula: C₁₇H₁₄ClNO₂S
• Molecular Weight: 331.823
• Mol file: 18392-55-7.mol

Synonyms:2-Naphthalenesulfonylchloride, 6-(N-methylanilino)- (8CI); 2,6-Mansyl chloride; N-Methyl-2-anilinonaphthalene-6-sulfonylchloride

Chemical Property of 2,6-mansyl chloride

Chemical Property:

• Vapor Pressure: 3.15E-10mmHg at 25°C
• Boiling Point: 502.5°Cat760mmHg
• Flash Point: 257.7°C
• PSA: 45.76000
• Density: 1.355g/cm³
• LogP: 5.61600

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-mansyl chloride

There total 2 articles about 2,6-mansyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(N-methylanilino)-naphthalene-6-sulfonic acid (23731-35-3) → 2,6-mansyl chloride (18392-55-7)

Guidance literature:

With trichlorophosphate; In pyridine;

DOI:10.1016/0022-2860(82)85259-9

Reference yield:

→ 2,6-mansyl chloride (18392-55-7)

Guidance literature:

Natrium-N-methyl-2-anilino-6-naphthalinsulfonat, POCl3;

DOI:10.1021/ja01008a041

Reference yield:

2,6-mansyl chloride (18392-55-7) + dimethyl amine (124-40-3) → 6-N-methyl-6-N-phenylamino-2-naphthalenesulfon-N,N-dimethylamide (61509-81-7)

Guidance literature:

In water;

DOI:10.1016/0022-2860(82)85259-9

upstream raw materials:

2-(N-methylanilino)-naphthalene-6-sulfonic acid

Downstream raw materials:

12-<6-(N-methylanilino)-2-naphtalenesulfonyloxy>-stearic acid

6-N-methyl-6-N-phenylamino-2-naphthalenesulfon-N,N-dimethylamide

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