Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester

Base Information

• Chemical Name: Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester
• CAS No.: 130694-58-5
• Molecular Formula: C₁₇H₂₄O₄
• Molecular Weight: 292.375

Synonyms:Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester

Chemical Property of Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester

Chemical Property:

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Technology Process of Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester

There total 18 articles about Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(-)-1(Z)-(1S,4R,6R)-1-(5-acetoxy-3-methylpent-3-en-1-ynyl)-2,2,6-trimethylcyclohexan-1,4-diol (130646-72-9) → Acetic acid (Z)-5-((1S,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester (26533-74-4,95343-50-3,95343-62-7,130694-58-5,130694-70-1,151004-76-1)

Guidance literature:

With dipyridinium dichromate; In dichloromethane; for 5h; Ambient temperature;

Reference yield: 70.0%

(-)-1(Z)-(1R,4R,6R)-1-(5-acetoxy-3-methylpent-3-en-1-ynyl)-2,2,6-trimethylcyclohexan-1,4-diol (130646-73-0) → Acetic acid (Z)-5-((1R,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester (130694-58-5)

Guidance literature:

With dipyridinium dichromate; In dichloromethane; for 5h; Ambient temperature;

Reference yield: 29.0%

sodium acetate (127-09-3) + acetic acid (64-19-7,77671-22-8) + 2-trans-5-(4',4'-ethylenedioxy-1'-hydroxy-2',2',6'-trimethylcyclohexyl)-3-methylpent-2-en-4-yn-1-ol (95307-31-6,95343-60-5,137432-90-7) → 2-trans-5-(1'-hydroxy-2',2',6'-trimethyl-4'-oxocyclohexyl)-3-methylpent-2-en-4-yn-1-ol (49846-56-2,70954-44-8,95343-49-0,95343-61-6,130694-57-4,130694-71-2,130694-74-5,137432-91-8,137432-93-0) + Acetic acid (E)-5-((1S,6R)-1-hydroxy-2,2,6-trimethyl-4-oxo-cyclohexyl)-3-methyl-pent-2-en-4-ynyl ester (26533-74-4,95343-50-3,95343-62-7,130694-58-5,130694-70-1,151004-76-1)

Guidance literature:

Heating;

upstream raw materials:

(-)-1(Z)-(1R,4R,6R)-1-(5-acetoxy-3-methylpent-3-en-1-ynyl)-2,2,6-trimethylcyclohexan-1,4-diol

(Z)-3-methylpent-2-en-4-ynol

(4R,6R)-4-hydroxy-2,2,6-trimethylcyclohexan-1-one

(6R)-levodione

Downstream raw materials:

(-)-4(Z)-(4R,5R)-4-hydroxy-4-(5-hydroxy-3-methylpent-3-en-1-ynyl)-3,3,5-trimethylcyclohexanone

(-)-4(1E,3Z)-(4S,5R)-4-hydroxy-4-(5-hydroxy-3-methyl-1,3-pentadienyl)-3,3,5-trimethylcyclohexanone

(-)-4(1E,3Z)-(4S,5R)-4-hydroxy-4-(3-methyl-5-oxo-1,3-pentadienyl)-3,3,5-trimethylcyclohexanone

(-)-(4S,5R)-dihydroabscisic acid

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