1,1'-(2,6-Naphthylene)bis(1-methylethanol)

Base Information

• Chemical Name: 1,1'-(2,6-Naphthylene)bis(1-methylethanol)
• CAS No.: 24157-82-2
• Molecular Formula: C₁₆H₂₀O₂
• Molecular Weight: 244.334
• Mol file: 24157-82-2.mol

Synonyms:2,6-Naphthalenedimethanol,a,a,a',a'-tetramethyl- (8CI,9CI);2,6-Bis(2-hydroxy-2-propyl)naphthalene; a,a'-Dihydroxy-2,6-diisopropylnaphthalene

Chemical Property of 1,1'-(2,6-Naphthylene)bis(1-methylethanol)

Chemical Property:

• Boiling Point: 415.6±25.0 °C(Predicted)
• PKA: 14.18±0.29(Predicted)
• Flash Point: 196.4oC
• PSA: 40.46000
• Density: 1.116±0.06 g/cm3(Predicted)
• LogP: 3.29460

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1'-(2,6-Naphthylene)bis(1-methylethanol)

There total 5 articles about 1,1'-(2,6-Naphthylene)bis(1-methylethanol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,6-diisopropylnaphthalene (24157-81-1) → 2,6-bis(2-hydroxy-2-propyl)naphthalene (24157-82-2)

Guidance literature:

With N-hydroxyphthalimide; oxygen; cobalt(II) diacetate tetrahydrate; In acetonitrile; at 40 ℃;

DOI:10.1021/op034137w

Reference yield:

2-(2-hydroxy-2-methylethyl)-6-(2-methylethyl)naphthalene (83922-21-8) → 2,6-bis(2-hydroxy-2-propyl)naphthalene (24157-82-2) + 2-(2-hydroperoxy-2-methylethyl)-6-(2-hydroxy-2-methylethyl)naphthalene

Guidance literature:

With sodium hydroxide; oxygen; 1-hexadecylcarboxylic acid; CuCN; In water; at 90 ℃; for 27h; under 760 Torr;

DOI:10.1002/(sici)1097-458x(200003)38:3<213::aid-mrc617>3.0.co;2-g

Reference yield:

2,6-bis(1-hydroperoxy-1-methylethyl)naphthalene (96783-79-8) → 2,6-bis(2-hydroxy-2-propyl)naphthalene (24157-82-2)

Guidance literature:

With sodium sulfite; In ethanol; water; at 40 ℃; for 3h;

DOI:10.1002/(sici)1097-458x(200003)38:3<213::aid-mrc617>3.0.co;2-g

upstream raw materials:

2-(2-hydroxy-2-methylethyl)-6-(2-methylethyl)naphthalene

2,6-bis(1-hydroperoxy-1-methylethyl)naphthalene

2-(1-hydroperoxy-1-methylethyl)-6-(1-methylethyl)naphthalene

2,6-diisopropylnaphthalene

Downstream raw materials:

2.6-dihydroxynaphthalene