(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

Base Information

Chemical Name:(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid
CAS No.:1560678-59-2
Molecular Formula:C₆H₆O₃S*C₂₅H₂₇N₃O₅
Molecular Weight:607.684
Hs Code.:

Synonyms:(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

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Chemical Property of (S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

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Technology Process of (S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

There total 6 articles about (S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1560609-43-9
(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

: 1560678-59-2
(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

Guidance literature:: With benzenesulfonic acid; In acetonitrile; Dean-Stark; Inert atmosphere;

Reference yield:

: 1560678-56-9
tert-butyl (4S)-5-amino-4-[4-[tert-butyl(dimethyl)silyl]oxy-1-oxo-isoindolin-2-yl]-5-oxo-pentanoate

: 1560678-59-2
(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / methanol / 15 - 25 °C

2: potassium carbonate / N,N-dimethyl-formamide / 25 - 50 °C

3: benzenesulfonic acid / acetonitrile / Dean-Stark; Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; benzenesulfonic acid; In methanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 359629-73-5
3-(tert-butyl-dimethyl-silanyloxy)-2-methyl-benzoic acid methyl ester

: 1560678-59-2
(S)-3-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)piperidine-2,6-dione besylate benzenesulfonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 45 - 50 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / methanol / 15 - 25 °C

3: potassium carbonate / N,N-dimethyl-formamide / 25 - 50 °C

4: benzenesulfonic acid / acetonitrile / Dean-Stark; Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; benzenesulfonic acid; In methanol; N,N-dimethyl-formamide; acetonitrile;