(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

Base Information

Chemical Name:(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate
CAS No.:1560609-43-9
Molecular Formula:C₂₉H₃₇N₃O₆
Molecular Weight:523.629
Hs Code.:

Synonyms:(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

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Chemical Property of (S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

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Technology Process of (S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

There total 4 articles about (S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1560678-56-9
tert-butyl (4S)-5-amino-4-[4-[tert-butyl(dimethyl)silyl]oxy-1-oxo-isoindolin-2-yl]-5-oxo-pentanoate

: 1560609-43-9
(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / methanol / 15 - 25 °C

2: potassium carbonate / N,N-dimethyl-formamide / 25 - 50 °C

With tetrabutyl ammonium fluoride; potassium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 603-80-5
3-hydroxy 2-methylbenzoic acid

: 1560609-43-9
(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 60 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 5 - 20 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 45 - 50 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride / methanol / 15 - 25 °C

5: potassium carbonate / N,N-dimethyl-formamide / 25 - 50 °C

With 1H-imidazole; sulfuric acid; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 55289-05-9
methyl 3-hydroxy-2-methylbenzoate

: 1560609-43-9
(S)-tert-butyl 5-amino-4-(4-((4-(morpholinomethyl)benzyl)oxy)-1-oxoisoindolin-2-yl)-5-oxopentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 3 h / 5 - 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 45 - 50 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / methanol / 15 - 25 °C

4: potassium carbonate / N,N-dimethyl-formamide / 25 - 50 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; acetonitrile;