5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Base Information

Chemical Name:5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide
CAS No.:1608112-47-5
Molecular Formula:C₂₃H₂₄BrNO₆
Molecular Weight:490.351
Hs Code.:

Synonyms:5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Suppliers and Price of 5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

There total 4 articles about 5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1608112-77-1
5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

: 1608112-47-5
5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201301238 DOI:10.1002/ejoc.201301238

Reference yield:

: C₁₂H₆BrClO₃

: 1608112-47-5
5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; In methanol;
DOI:10.1002/ejoc.201301238

Reference yield:

: 60907-47-3
C₁₂H₇BrO₄

: 1608112-47-5
5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / Reflux; Inert atmosphere

2: triethylamine / Inert atmosphere

3: sodium tetrahydroborate / methanol / 1 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; thionyl chloride; triethylamine; In methanol;
DOI:10.1002/ejoc.201301238