5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Base Information

Chemical Name:5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide
CAS No.:1608112-77-1
Molecular Formula:C₂₃H₂₂BrNO₆
Molecular Weight:488.335
Hs Code.:

Synonyms:5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

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Chemical Property of 5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

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Technology Process of 5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

There total 2 articles about 5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60907-47-3
C₁₂H₇BrO₄

: 1608112-77-1
5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / Reflux; Inert atmosphere

2: triethylamine / Inert atmosphere

With thionyl chloride; triethylamine;
DOI:10.1002/ejoc.201301238

Reference yield:

: C₁₂H₆BrClO₃

: 163629-15-0
N-ethyl-3,4,5-trimethoxyaniline

: 1608112-77-1
5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: With triethylamine; Inert atmosphere;
DOI:10.1002/ejoc.201301238

Reference yield: 75.0%

: 1608112-77-1
5-(2-bromobenzoyl)furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

: 1608112-47-5
5-[(2-bromophenyl)-hydroxy-methyl]-furan-2-carboxylic acid ethyl-(3,4,5-trimethoxyphenyl)amide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201301238 DOI:10.1002/ejoc.201301238