Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate

Base Information

Chemical Name:Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate
CAS No.:151071-04-4
Molecular Formula:C₁₃H₁₅IO₂
Molecular Weight:330.165
Hs Code.:
DSSTox Substance ID:DTXSID401220897

Synonyms:SCHEMBL20472134;DTXSID401220897;Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate;151071-04-4

Suppliers and Price of Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:330.01168
Heavy Atom Count:16
Complexity:269

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCC1=C(C=CC(=C1)I)OC(=O)C)C

Technology Process of Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate

There total 5 articles about Phenol, 4-iodo-2-(3-methyl-2-buten-1-yl)-, 1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-36-5
acetyl chloride

: 151071-03-3
4-iodo-2-(3-methylbut-2-en-1-yl)phenol

: 151071-04-4
4-iodo-2-(3-methylbut-2-en-1-yl)phenyl acetate

Guidance literature:: With dmap; In dichloromethane; for 4h; Heating;
DOI:10.1016/j.bmc.2006.04.015

Reference yield: 92.0%

: 151071-04-4
4-iodo-2-(3-methylbut-2-en-1-yl)phenyl acetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 870-63-3
prenyl bromide

: 151071-04-4
4-iodo-2-(3-methylbut-2-en-1-yl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaH / toluene / 1 h / 20 °C

2: 96 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 4 h / Heating

With dmap; sodium hydride; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2006.04.015