diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

Base Information

Chemical Name:diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate
CAS No.:1447961-16-1
Molecular Formula:C₃₀H₃₃Cl₂N₄O₅P
Molecular Weight:631.496
Hs Code.:

Synonyms:diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

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Chemical Property of diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

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Technology Process of diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

There total 4 articles about diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 884489-32-1
[3-benzyloxyamino-1-(3,4-dichlorophenyl)-propyl]-phosphonic acid diethyl ester

: 857284-23-2
3-[(1H-1,2,4-triazol-1-yl)methyl]benzoic acid

: 1447961-16-1
diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

Guidance literature:: With C₅H₉O₆P; triethylamine; In ethyl acetate; at 20 ℃; for 3h;
DOI:10.1021/jm4006498

Reference yield:

: 151169-75-4
3,4-dichlophenylboronic acid

: 1447961-16-1
diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; p-benzoquinone; 2.9-dimethyl-1,10-phenanthroline / 100 °C / Microwave irradiation

2.1: phenol / 100 °C

2.2: 100 °C

3.1: pyridine / ethanol / 20 °C

3.2: 20 °C

4.1: triethylamine; C₅H₉O₆P / ethyl acetate / 3 h / 20 °C

With pyridine; 2.9-dimethyl-1,10-phenanthroline; C₅H₉O₆P; palladium diacetate; triethylamine; p-benzoquinone; phenol; In ethanol; ethyl acetate; 1.1: |Heck Reaction;
DOI:10.1021/jm4006498

Reference yield:

: 62374-02-1
(E)-3,4-dichlorocinnamaldehyde

: 1447961-16-1
diethyl (3-(3-((1H-1,2,4-triazol-1-yl)methyl)-N-(benzyloxy)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: phenol / 100 °C

1.2: 100 °C

2.1: pyridine / ethanol / 20 °C

2.2: 20 °C

3.1: triethylamine; C₅H₉O₆P / ethyl acetate / 3 h / 20 °C

With pyridine; C₅H₉O₆P; triethylamine; phenol; In ethanol; ethyl acetate;
DOI:10.1021/jm4006498