5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine

Base Information

• Chemical Name: 5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine
• CAS No.: 1094601-71-4
• Molecular Formula: C₃₅H₄₃FN₄O₄Si
• Molecular Weight: 630.835

Synonyms:5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine

Chemical Property of 5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine

Chemical Property:

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Technology Process of 5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine

There total 1 articles about 5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)uridine (1094601-70-3) → 5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine (1094601-71-4)

Guidance literature:

5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)uridine; With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine; In acetonitrile; at 20 ℃; for 1h;

With ammonium hydroxide; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2008.08.117

Reference yield:

5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)cytidine (1094601-71-4) + benzoyl chloride (98-88-4) → C42H47FN4O5Si

Guidance literature:

With pyridine; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2008.08.117

upstream raw materials:

5'-amino-3'-O-(tert-butyldimethylsilyl)-2',5'-dideoxy-2'-fuoro-5'-N-(4'-monomethoxytrityl)uridine

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