[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

Base Information

Chemical Name:[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten
CAS No.:82281-49-0
Molecular Formula:C₁₇H₁₅O₅PW
Molecular Weight:514.127
Hs Code.:

Synonyms:[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

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Chemical Property of [1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

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Technology Process of [1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

There total 5 articles about [1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 852242-57-0
3-phenyl-3H-3-benzophosphenine pentacarbonyltungsten⁽⁰⁾

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 82281-49-0
[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

: P(C₆H₅)W(CO)5CH₂CHC(CH₃)CH₂

Guidance literature:: In further solvent(s); complex C10H8P(C6H5)W(CO)5 reacted with butadiene at 75-80°C;
DOI:10.1021/ja050817y

Reference yield: 63.0%

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 82281-49-0
[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

Guidance literature:: In toluene; 16-17 h at 150°C; chromy. (silica gel, hexane/toluene); elem. anal.;
DOI:10.1021/ja00380a029

Reference yield: 44.0%

: 88080-18-6,88000-36-6
[1-phenyl-2-methyl-2-(1-methylvinyl)phosphirane]pentacarbonyltungsten

: 82281-49-0
[1-phenyl-3,4-dimethylphospholene](pentacarbonyl)tungsten

Guidance literature:: In toluene; Heating in toluene at 95°C for 24 h or at 105°C for 3 h (Ar atm.);; evapd., chromd. on silica column with hexane under Ar atm.; elem. anal.;;
DOI:10.1021/om00081a021