Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Base Information

Chemical Name:Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate
CAS No.:1415043-05-8
Molecular Formula:C₂₅H₂₆N₂O₅S
Molecular Weight:466.558
Hs Code.:

Synonyms:Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Chemical Property of Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Technology Process of Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

There total 12 articles about Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1415043-02-5
tert-Butyl 1-(2-ethoxy-2-oxoethyl)-2-methyl-4-oxo-3-[2-(phenylsulfonyl)benzyl]-1,4,6,7-tetra hydro-5H-pyrrolo[3,2-c]pyridine-5-carboxylate

: 1415043-05-8
Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Product distribution / selectivity;

Reference yield: 61.0%

: 1415042-82-8
tert-butyl 1-(2-ethoxy-2-oxoethyl)-2-methyl-4-oxo-1,4,6,7-tetrahydro-5H-pyrrolo[3,2-c]pyridine-5-carboxylate

: 126076-76-4
2-(phenylsulfonyl)benzaldehyde

: 1415043-05-8
Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: With water; hydrogen iodide; hypophosphorous acid; acetic anhydride; at 20 ℃; for 1.5h; Product distribution / selectivity;

Reference yield:

: 446-52-6
2-Fluorobenzaldehyde

: 1415043-05-8
Ethyl 2-(2-methyl-4-oxo-3-(2-(phenylsulfonyl)benzyl)-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 4 h / 100 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

3: acetic anhydride; hypophosphorous acid; water; hydrogen iodide / 1.5 h / 20 °C

With water; hydrogen iodide; hypophosphorous acid; acetic anhydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; dimethyl sulfoxide;