t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

Base Information

Chemical Name:t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate
CAS No.:1132660-85-5
Molecular Formula:C₂₆H₃₃N₃O₆
Molecular Weight:483.565
Hs Code.:

Synonyms:t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

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Chemical Property of t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

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Technology Process of t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

There total 1 articles about t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1132660-84-4
2-(3-amino-4-hydroxyphenyl)-5,7-dimethoxy-1-methylquinolin-4(1H)-one

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1132660-85-5
t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/j.bmcl.2008.12.034

Reference yield: 77.0%

: 3724-19-4
3-pyridine propionic acid

: 1132660-85-5
t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

: 1132660-87-7
t-butyl 3-{4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)-2-[(3-pyridin-3-ylpropanoyl)amino]phenoxy}propylcarbamate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.bmcl.2008.12.034

Reference yield: 57.0%

: 1132660-85-5
t-butyl 3-[2-amino-4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)phenoxy]propyl carbamate

: 69954-66-1
4-(dimethylamino)butyric acid hydrochloride

: 1132660-86-6
t-butyl 3-(4-(5,7-dimethoxy-1-methyl-4-oxo-1,4-dihydroquinolin-2-yl)-2-{[4-(dimethylamino)butanoyl]amino}phenoxy)propylcarbamate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 50 ℃; for 4h;
DOI:10.1016/j.bmcl.2008.12.034