3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

Base Information

Chemical Name:3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride
CAS No.:1255149-56-4
Molecular Formula:C₁₈H₁₄N₄O₆*ClH
Molecular Weight:418.793
Hs Code.:

Synonyms:3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

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Chemical Property of 3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

Chemical Property:

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Technology Process of 3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

There total 8 articles about 3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255149-59-7
C₂₀H₁₈N₄O₇*ClH

: 1255149-56-4
3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; isopropyl alcohol; at 20 ℃; for 8h;

Reference yield:

: 405277-41-0
4-(4,4,5,5-tetramethyl-1,3-dioxolan-2-yl)aniline

: 1255149-56-4
3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 48 h / Reflux; Inert atmosphere

2.1: hydrazine / 1,4-dioxane; ethanol / 6 h / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C

4.1: hydrogenchloride / isopropyl alcohol; 1,4-dioxane; tetrahydrofuran / 8 h / 20 °C

With hydrogenchloride; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 32460-07-4
ethyl 3-bromofuran-2-carboxylate

: 1255149-56-4
3-(4-aminophenyl)-2-furan carboxylic acid 2-(4-hydroxy-3-nitrobenzoyl)hydrazide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 48 h / Reflux; Inert atmosphere

2.1: hydrazine / 1,4-dioxane; ethanol / 6 h / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C

4.1: hydrogenchloride / isopropyl alcohol; 1,4-dioxane; tetrahydrofuran / 8 h / 20 °C

With hydrogenchloride; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydrazine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol;