C₂₈H₄₆N₈O₇S

Base Information

Chemical Name:C₂₈H₄₆N₈O₇S
CAS No.:260270-92-6
Molecular Formula:C₂₈H₄₆N₈O₇S
Molecular Weight:638.789
Hs Code.:

C<sub>28</sub>H<sub>46</sub>N<sub>8</sub>O<sub>7</sub>S

Synonyms:C₂₈H₄₆N₈O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₄₆N₈O₇S

Chemical Property:

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Technology Process of C₂₈H₄₆N₈O₇S

There total 11 articles about C₂₈H₄₆N₈O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 212610-30-5
(2R,3S)-2-(cyclohexylmethyl)-3-[formyl(tetrahydro-2H-pyran-2-yloxy)amino]hexanoic acid

: L-N^G-nitroarginine 2-aminothiazole amide dihydrochloride

: 260270-92-6
C₂₈H₄₆N₈O₇S

Guidance literature:: (2R,3S)-2-(cyclohexylmethyl)-3-[formyl(tetrahydro-2H-pyran-2-yloxy)amino]hexanoic acid; With 4-methyl-morpholine; diethyl cyanophosphonate; In N,N-dimethyl-formamide; at 0 - 20 ℃;

L-N^G-nitroarginine 2-aminothiazole amide dihydrochloride; With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 23 - 40 ℃; Further stages.;
DOI:10.1021/jm0102654

Reference yield:

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 260270-92-6
C₂₈H₄₆N₈O₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: DCC / ethyl acetate / 0 - 20 °C

2.1: pyridine / CH₂Cl₂ / 0 °C

3.1: K₂CO₃ / acetone / 12 h / Heating

4.1: aq. NaOH / dioxane / 24 h / 25 °C

5.1: pyridine / CH₂Cl₂ / 2 h / 0 °C

6.1: diethyl phosphorylcyanide; NMM / dimethylformamide / 0 - 20 °C

6.2: NMM / dimethylformamide / 23 - 40 °C

With 4-methyl-morpholine; pyridine; sodium hydroxide; diethyl cyanophosphonate; potassium carbonate; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm0102654

Reference yield:

: 109053-86-3
methyl (3R)-3-hydroxyhexanoate

: 260270-92-6
C₂₈H₄₆N₈O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: 45 percent / LDA; DMPU / tetrahydrofuran / -78 - 0 °C

2.1: aq. LiOH / tetrahydrofuran; methanol / 24 h

3.1: DCC / ethyl acetate / 0 - 20 °C

4.1: pyridine / CH₂Cl₂ / 0 °C

5.1: K₂CO₃ / acetone / 12 h / Heating

6.1: aq. NaOH / dioxane / 24 h / 25 °C

7.1: pyridine / CH₂Cl₂ / 2 h / 0 °C

8.1: diethyl phosphorylcyanide; NMM / dimethylformamide / 0 - 20 °C

8.2: NMM / dimethylformamide / 23 - 40 °C

With 4-methyl-morpholine; pyridine; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hydroxide; sodium hydroxide; diethyl cyanophosphonate; potassium carbonate; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; 1.1: Frater-Seebach alkylation;
DOI:10.1021/jm0102654