methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

Base Information

Chemical Name:methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate
CAS No.:233755-55-0
Molecular Formula:C₂₆H₂₅ClN₂O₇S
Molecular Weight:545.013
Hs Code.:

Synonyms:methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

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Chemical Property of methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

Chemical Property:

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Technology Process of methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

There total 4 articles about methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38870-89-2
Methoxyacetyl chloride

: 522623-56-9
methyl 2-{(2-aminobenzyl)-[4-(4-chlorophenyloxy)benzene-sulfonyl]amino}-3-hydroxypropionate

: 233755-55-0
methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0960-894X(02)00633-9

Reference yield:

: 191327-30-7
4-(4'-chlorophenoxy)phenylsulfonyl chloride

: 233755-55-0
methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂

2: NaH / dimethylformamide

3: ammonium formate / 10 percent Pd/C / ethanol

4: Et₃N / CH₂Cl₂

With ammonium formate; sodium hydride; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00633-9

Reference yield:

: 522623-54-7
2-[4-(4-chloro-phenoxy)-benzenesulfonylamino]-3-hydroxy-propionic acid methyl ester

: 233755-55-0
methyl 2-{[4-(4-chlorophenyloxy)benzenesulfonyl]-[2-(methoxyacetylamino)benzyl]amino}acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: ammonium formate / 10 percent Pd/C / ethanol

3: Et₃N / CH₂Cl₂

With ammonium formate; sodium hydride; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00633-9