9-(4-(bromomethyl)phenyl)-9H-carbazole

Base Information

Chemical Name:9-(4-(bromomethyl)phenyl)-9H-carbazole
CAS No.:845659-67-8
Molecular Formula:C₁₉H₁₄BrN
Molecular Weight:336.231
Hs Code.:

Synonyms:9-(4-(bromomethyl)phenyl)-9H-carbazole

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Chemical Property of 9-(4-(bromomethyl)phenyl)-9H-carbazole

Chemical Property:

Boiling Point:475.6±37.0 °C(Predicted)
Density:1.35±0.1 g/cm3(Predicted)

Purity/Quality:

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Technology Process of 9-(4-(bromomethyl)phenyl)-9H-carbazole

There total 6 articles about 9-(4-(bromomethyl)phenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 19264-73-4
9-(4-methylphenyl)-9H-carbazole

: 845659-67-8
9-(4-(bromomethyl)phenyl)-9H-carbazole

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 3h; Inert atmosphere; Reflux;
DOI:10.1071/CH13521

Reference yield: 57.0%

: 71935-22-3
[4‐(9H‐carbazol‐9‐yl)phenyl]methanol

: 845659-67-8
9-(4-(bromomethyl)phenyl)-9H-carbazole

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 845659-67-8
9-(4-(bromomethyl)phenyl)-9H-carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: tri-tert-butyl phosphine; palladium diacetate; potassium carbonate / toluene / 24 h / 115 °C

2: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C

3: phosphorus tribromide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; tri-tert-butyl phosphine; palladium diacetate; phosphorus tribromide; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; toluene;
DOI:10.1016/j.saa.2012.11.022