3-(9H-Carbazole-9-yl)benzyl alcohol

Base Information

Chemical Name:3-(9H-Carbazole-9-yl)benzyl alcohol
CAS No.:71935-22-3
Molecular Formula:C19H15 N O
Molecular Weight:273.334
Hs Code.:
Mol file:71935-22-3.mol

Synonyms:[4-(9H-Carbazol-9-yl)phenyl]methanol

Suppliers and Price of 3-(9H-Carbazole-9-yl)benzyl alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-(9H-Carbazole-9-yl)benzyl alcohol

Chemical Property:

PSA：25.16000
LogP:4.27600

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(9H-Carbazole-9-yl)benzyl alcohol

There total 7 articles about 3-(9H-Carbazole-9-yl)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 110677-45-7
N-(4-formylphenyl)carbazole

: 71935-22-3
[4‐(9H‐carbazol‐9‐yl)phenyl]methanol

Guidance literature:: With methanol; sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield: 82.0%

: 873-75-6
4-bromobenzenemethanol

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 71935-22-3
[4‐(9H‐carbazol‐9‐yl)phenyl]methanol

Guidance literature:: With copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; potassium carbonate; In dimethyl sulfoxide; at 130 ℃;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 71935-22-3
[4‐(9H‐carbazol‐9‐yl)phenyl]methanol

Guidance literature:: Multi-step reaction with 2 steps

1: tri-tert-butyl phosphine; palladium diacetate; potassium carbonate / toluene / 24 h / 115 °C

2: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C

With sodium tetrahydroborate; tri-tert-butyl phosphine; palladium diacetate; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; toluene;
DOI:10.1016/j.saa.2012.11.022