methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Base Information

Chemical Name:methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate
CAS No.:1369804-21-6
Molecular Formula:C₂₇H₂₆N₄O₅S
Molecular Weight:518.593
Hs Code.:

Synonyms:methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

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Chemical Property of methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

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Technology Process of methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

There total 5 articles about methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369804-19-2
methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

: 41994-93-8
6-methoxy-1,2,3-benzotriazin-4(3H)-one

: 1369804-21-6
methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 0.5h; Inert atmosphere;

Reference yield:

: 1369800-50-9
α-[(4-nitrophenyl)thio]-γ-butyrolactone

: 1369804-21-6
methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h

2: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3: sodium hydroxide / N,N-dimethyl-formamide; water / 0.5 h

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrogen; triethylamine; triphenylphosphine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1369804-21-6
methyl 4-(6-methoxy-4-oxo-1,2,3-benzotriazin-3(4H)-yl)-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h

3: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4: sodium hydroxide / N,N-dimethyl-formamide; water / 0.5 h

5: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrogen; triethylamine; triphenylphosphine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;