methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Base Information

Chemical Name:methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate
CAS No.:1369804-19-2
Molecular Formula:C₁₉H₂₁NO₄S
Molecular Weight:359.446
Hs Code.:

Synonyms:methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

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Chemical Property of methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Chemical Property:

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Technology Process of methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

There total 4 articles about methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1369804-17-0
4-methyl-N-{4-[(2-oxotetrahydrofuran-3-yl)sulfanyl]phenyl}benzamide

: 74-88-4
methyl iodide

: 1369804-19-2
methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: 4-methyl-N-{4-[(2-oxotetrahydrofuran-3-yl)sulfanyl]phenyl}benzamide; With sodium hydroxide; In water; N,N-dimethyl-formamide; for 0.5h;

methyl iodide; With sodium hydrogencarbonate; 18-crown-6 ether;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1369804-19-2
methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h

3: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4: sodium hydroxide / N,N-dimethyl-formamide; water / 0.5 h

With hydrogen; triethylamine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1369800-50-9
α-[(4-nitrophenyl)thio]-γ-butyrolactone

: 1369804-19-2
methyl 4-hydroxy-2-[(4-{[(4-methylphenyl)carbonyl]amino}phenyl)sulfanyl]butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium on activated charcoal / tetrahydrofuran; methanol / 2 h

2: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3: sodium hydroxide / N,N-dimethyl-formamide; water / 0.5 h

With hydrogen; triethylamine; sodium hydroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;