Technology Process of S-(5-(4-iodophenyl)pentyl) ethanethioate
There total 6 articles about S-(5-(4-iodophenyl)pentyl) ethanethioate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-(4-iodophenyl)pentyl methanesulfonate;
With
caesium carbonate;
In
N,N-dimethyl-formamide;
for 0.5h;
tiolacetic acid;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1021/ja411573a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 1.5 h / -20 - 20 °C
1.2: 16 h / 20 °C
2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h
2.2: 20 °C
With
caesium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja411573a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine / tert-butyl alcohol / 18 h / Reflux
2.1: triethylamine / dichloromethane / 1.5 h / -20 - 20 °C
2.2: 16 h / 20 °C
3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h
3.2: 20 °C
With
copper(l) iodide; caesium carbonate; triethylamine; sodium iodide; N,N`-dimethylethylenediamine;
In
dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja411573a
