thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

Base Information

Chemical Name:thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester
CAS No.:313254-02-3
Molecular Formula:C₁₇H₃₁O₃PSSi
Molecular Weight:374.557
Hs Code.:

thiophosphoric acid <i>S</i>-[(<i>tert</i>-butyl-dimethyl-silanyl)-phenyl-methyl] ester <i>O</i>,<i>O</i>'-diethyl ester

Synonyms:thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

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Chemical Property of thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

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Technology Process of thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

There total 3 articles about thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 762-04-9
phosphonic acid diethyl ester

: 313253-99-5
t-butyldimethylsilyl phenyl thioketone

: 313254-02-3
thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -98 ℃; for 1h;
DOI:10.1016/S0022-328X(00)00482-4

Reference yield: 18.0%

: 762-04-9
phosphonic acid diethyl ester

: 313253-99-5
t-butyldimethylsilyl phenyl thioketone

: 70660-07-0
(Mercapto-phenyl-methyl)-phosphonic acid diethyl ester

: 313254-02-3
thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

: [(tert-butyl-dimethyl-silanylsulfanyl)-phenyl-methyl]-phosphonic acid diethyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -98 ℃; for 0.5h;
DOI:10.1016/S0022-328X(00)00482-4

Reference yield:

: 132868-67-8
(tert-butyldimethylsilyl)(phenyl)methanone

: 313254-02-3
thiophosphoric acid S-[(tert-butyl-dimethyl-silanyl)-phenyl-methyl] ester O,O'-diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / hydrogen chloride; hydrogen sulfide / diethyl ether / 0.08 h / -10 °C

2: 19 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / -98 °C

With hydrogenchloride; n-butyllithium; hydrogen sulfide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/S0022-328X(00)00482-4