N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide

Base Information

• Chemical Name: N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide
• CAS No.: 1241555-63-4
• Molecular Formula: C₂₁H₁₉N₅O₃S
• Molecular Weight: 421.48

Synonyms:N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide

Chemical Property of N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide

Chemical Property:

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Technology Process of N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide

There total 2 articles about N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

2-methoxybenzylamine (6850-57-3) + C13H10N4O3S (1147760-51-7) → N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide (1241555-63-4)

Guidance literature:

C₁₃H₁₀N₄O₃S; With 1,1'-carbonyldiimidazole; In 1,4-dioxane; at 60 - 80 ℃; for 1h; Reflux;

2-methoxybenzylamine; In 1,4-dioxane; for 3h; Reflux;

DOI:10.1007/s00044-012-0257-x

Reference yield: 56.3%

C11H7N4OS(1-)*K(1+) (1258381-10-0) + 2-chloro-N-(2-methoxybenzyl)acetamide (81494-04-4) → N-(2-methoxybenzyl)-2-[(3-methyl-2-oxo-2H-[1,2,4]triazino[2,3-c]quinazoline-6-yl)thio]acetamide (1241555-63-4)

Guidance literature:

In isopropyl alcohol; for 1 - 1.5h; Reflux;

DOI:10.1007/s00044-012-0257-x

upstream raw materials:

2-methoxybenzylamine

C₁₃H₁₀N₄O₃S

C₁₁H₇N₄OS^(1-)*K⁽¹⁺⁾

2-chloro-N-(2-methoxybenzyl)acetamide

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