benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

Base Information

Chemical Name:benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester
CAS No.:690270-09-8
Molecular Formula:C₃₇H₂₈N₆O₉
Molecular Weight:700.664
Hs Code.:

Synonyms:benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

There total 10 articles about benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1365255-42-0
C₃₀H₂₃N₅O₉

: 98-88-4
benzoyl chloride

: 690270-09-8
benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

Guidance literature:: C₃₀H₂₃N₅O₉; With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine; In acetonitrile; at 20 ℃; for 14h;

With ammonia; In tetrahydrofuran; at 20 ℃; for 2h;

benzoyl chloride; With pyridine; at 20 ℃; for 16h;

Reference yield:

: 532-32-1
sodium benzoate

: 690270-09-8
benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 15-crown-5 / N,N-dimethyl-formamide / 120 h / 90 - 100 °C

2.1: dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine / acetonitrile / 14 h / 20 °C

2.2: 2 h / 20 °C

2.3: 16 h / 20 °C

With dmap; 2,4,6-triisopropylphenylsulfonyl chloride; 15-crown-5; triethylamine; In N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 98-88-4
benzoyl chloride

: 690270-09-8
benzoic acid (2R,3S,4R,5R)-2-azido-3,4-dibenzoyloxy-5-(4-benzoylamino-2-oxo-2H-pyrimidin-1-yl)-tetrahydrofuran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 14 h / 0 - 20 °C

2.1: dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine / acetonitrile / 14 h / 20 °C

2.2: 2 h / 20 °C

2.3: 16 h / 20 °C

With pyridine; dmap; 2,4,6-triisopropylphenylsulfonyl chloride; triethylamine; In acetonitrile;