C₂₇H₂₆FNO₇S

Base Information

Chemical Name:C₂₇H₂₆FNO₇S
CAS No.:1374234-41-9
Molecular Formula:C₂₇H₂₆FNO₇S
Molecular Weight:527.57
Hs Code.:

C<sub>27</sub>H<sub>26</sub>FNO<sub>7</sub>S

Synonyms:C₂₇H₂₆FNO₇S

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Chemical Property of C₂₇H₂₆FNO₇S

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Technology Process of C₂₇H₂₆FNO₇S

There total 7 articles about C₂₇H₂₆FNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1374234-40-8
C₂₆H₂₄FNO₅

: 124-63-0
methanesulfonyl chloride

: 1374234-41-9
C₂₇H₂₆FNO₇S

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 3h;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-41-9
C₂₇H₂₆FNO₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

7.1: pyridine / dichloromethane / 3 h / 0 °C

With pyridine; potassium phosphate; hydrogen; nitric acid; sodium hydride; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-41-9
C₂₇H₂₆FNO₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

6.1: pyridine / dichloromethane / 3 h / 0 °C

With pyridine; potassium phosphate; hydrogen; nitric acid; caesium carbonate; zinc(II) chloride; palladium 10% on activated carbon; palladium diacetate; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;