C₁₃H₁₀FNO

Base Information

Chemical Name:C₁₃H₁₀FNO
CAS No.:1201761-95-6
Molecular Formula:C₁₃H₁₀FNO
Molecular Weight:215.227
Hs Code.:

Synonyms:C₁₃H₁₀FNO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₀FNO

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Technology Process of C₁₃H₁₀FNO

There total 1 articles about C₁₃H₁₀FNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 109-97-7,30604-81-0
pyrrole

: 13565-08-7,39098-89-0
4-fluorocinnamoyl chloride

: 1201761-95-6
C₁₃H₁₀FNO

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; at 25 ℃; for 12h;
DOI:10.1021/acs.joc.8b00831

Reference yield: 99.0%

: 1201761-95-6
C₁₃H₁₀FNO

: 7215-33-0
diethylphosphine oxide

: 1221726-83-5
(S)-3-(diethylphosphoryl)-3-(4-fluorophenyl)-1-pyrrol-1-yl-propan-1-one

Guidance literature:: With pyridine; dimethyl zinc(II); ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol); In toluene; at 0 - 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol100504h

Reference yield: 96.0%

: 1201761-95-6
C₁₃H₁₀FNO

: 762-04-9
phosphonic acid diethyl ester

: 1201762-16-4
(S)-diethyl 1-(4-fluorophenyl)-3-oxo-3-pyrrol-1-yl-propylphosphonate

Guidance literature:: With diethylzinc; ((2S,2'S)-((2-hydroxy-5-methyl-1,3-phenylene)bis(methylene))bis(pyrrolidine-1,2-diyl))bis(diphenylmethanol); In toluene; at 0 - 20 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.200901901