ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

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Chemical Name:ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate
CAS No.:866640-85-9
Molecular Formula:C₃₂H₄₂N₂O₆
Molecular Weight:550.695
Hs Code.:

Synonyms:ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

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Chemical Property of ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

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Technology Process of ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

There total 4 articles about ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 866640-84-8
ethyl 2-(4-{[(2-tert-butoxy-2-oxoethyl)amino]methyl}-2,6-dimethylphenoxy)-2-methylpropanoate

: 103788-61-0
(5-methyl-2-phenyl-4-oxazolyl)methyl chloride

: 866640-85-9
ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

Guidance literature:: With potassium carbonate; In acetonitrile; for 24h; Reflux;
DOI:10.1248/cpb.c13-00513

Reference yield:

: 639784-17-1
ethyl 2-(4-formyl-2,6-dimethylphenoxy)-2-methylpropanoate

: 866640-85-9
ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / tetrahydrofuran / 4 h / Reflux

2: sodium tetrahydroborate / methanol / 4 h / 0 - 20 °C

3: potassium carbonate / acetonitrile / 24 h / Reflux

With sodium tetrahydroborate; magnesium sulfate; potassium carbonate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1248/cpb.c13-00513

Reference yield:

: C₂₁H₃₁NO₅

: 866640-85-9
ethyl 2-[4-({(2-tert-butoxy-2-oxoethyl)[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methyl]amino}methyl)-2,6-dimethylphenoxy]-2-methylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 4 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 24 h / Reflux

With sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;
DOI:10.1248/cpb.c13-00513