FeCl₃{((CH₃O)3C₆H₂)3PO}

Base Information

Chemical Name:FeCl₃{((CH₃O)3C₆H₂)3PO}
CAS No.:131329-88-9
Molecular Formula:C₂₇H₃₃Cl₃FeO₁₀P
Molecular Weight:710.733
Hs Code.:

FeCl<sub>3</sub>{((CH<sub>3</sub>O)3C<sub>6</sub>H<sub>2</sub>)3PO}

Synonyms:FeCl₃{((CH₃O)3C₆H₂)3PO}

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Chemical Property of FeCl₃{((CH₃O)3C₆H₂)3PO}

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Technology Process of FeCl₃{((CH₃O)3C₆H₂)3PO}

There total 6 articles about FeCl₃{((CH₃O)3C₆H₂)3PO} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: Fe⁽³⁺⁾*3Cl^(1-)*((CH₃O)3C₆H₂)3P=FeCl₃((CH₃O)3C₆H₂)3P

: 131329-88-9
FeCl₃{((CH₃O)3C₆H₂)3PO}

Guidance literature:: With O₂; In dichloromethane; under Ar, bubbling dry O2 through a soln. of FeCl3(TMPP), 1 h, room temp., further exposing to O2 (> 12 h);; vac. evapn., elem. anal.;
DOI:10.1016/S0277-5387(00)83974-1

Reference yield: 81.0%

: 7705-08-0
iron(III) chloride

: 148345-92-0
tris(2,4,6-trimethoxyphenyl)phosphine oxide

: 131329-88-9
FeCl₃{((CH₃O)3C₆H₂)3PO}

Guidance literature:: In ethanol; undee Ar, addn. of ligand in EtOH to FeCl3, orange suspn. stirred at room temp. for 1 h until dissolution of FeCl3; filtered in air, washed with EtOH and Et2O, dried in vac.;
DOI:10.1016/S0277-5387(00)81763-5

Reference yield: 80.0%

: 2PH(C₆H₂(OCH₃)3)3⁽¹⁺⁾*Fe₂Cl₆^(2-)={PH(C₆H₂(OCH₃)3)3}2{Fe₂Cl₆}

: 131329-88-9
FeCl₃{((CH₃O)3C₆H₂)3PO}

Guidance literature:: With oxygen; In ethanol; dry O2 bubbled through yellow soln. for 10 min, color changed to dark orange; evapd. under a purge of O2, pptn.; elem. anal.;
DOI:10.1016/S0277-5387(00)81763-5