2,2-Dichloro-N-acetamide

Base Information

• Chemical Name: 2,2-Dichloro-N-acetamide
• CAS No.: 133901-67-4
• Molecular Formula: C₁₆H₁₃Cl₂NO
• Molecular Weight: 306.191

Synonyms:2,2-Dichloro-N-acetamide

Chemical Property of 2,2-Dichloro-N-acetamide

Chemical Property:

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Technology Process of 2,2-Dichloro-N-acetamide

There total 1 articles about 2,2-Dichloro-N-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

dichloroacethyl chloride (79-36-7) + 2-(1-phenylvinyl)aniline (64097-92-3) → 2,2-Dichloro-N-acetamide (133901-67-4)

Guidance literature:

With triethylamine; In diethyl ether; for 0.166667h; Ambient temperature;

Reference yield: 33.0%

2,2-Dichloro-N-acetamide (133901-67-4) → 2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-(1)-benzazepine (16140-89-9) + N-[2-(1-phenylethenyl)phenyl]acetamide (133901-52-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 3h; Heating;

upstream raw materials:

dichloroacethyl chloride

2-(1-phenylvinyl)aniline

Downstream raw materials:

2-oxo-5-phenyl-2,3,4,5-tetrahydro-1H-⁽¹⁾-benzazepine

N-[2-(1-phenylethenyl)phenyl]acetamide

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