alpha-(2-Methylpropylidene)pyridine-2-acetonitrile

Base Information

Chemical Name:alpha-(2-Methylpropylidene)pyridine-2-acetonitrile
CAS No.:22346-07-2
Molecular Formula:C11H12 N2
Molecular Weight:172.23
Hs Code.:2933399090
European Community (EC) Number:244-923-9
DSSTox Substance ID:DTXSID00944995
Mol file:22346-07-2.mol

Synonyms:alpha-(2-Methylpropylidene)pyridine-2-acetonitrile;4-methyl-2-pyridin-2-ylpent-2-enenitrile;EINECS 244-923-9;22346-07-2;SCHEMBL11234112;DTXSID00944995;4-methyl 2-(2-pyridyl) 2-pentene nitrile

Suppliers and Price of alpha-(2-Methylpropylidene)pyridine-2-acetonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of alpha-(2-Methylpropylidene)pyridine-2-acetonitrile

Chemical Property:

Boiling Point:293.4°Cat760mmHg
Flash Point:108.1°C
PSA：36.68000
Density:1.011g/cm³
LogP:2.64458
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:172.100048391
Heavy Atom Count:13
Complexity:232

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C=C(C#N)C1=CC=CC=N1

Technology Process of alpha-(2-Methylpropylidene)pyridine-2-acetonitrile

There total 3 articles about alpha-(2-Methylpropylidene)pyridine-2-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2739-97-1
pyridine-2-acetonitrile

: 78-84-2
isobutyraldehyde

: 22346-07-2
4-methyl-2-(2-pirydyl)-2-pentenenitrile

Guidance literature:: With piperidine; acetic acid; In benzene; for 3h; Heating;
DOI:10.1021/jm00357a026

Reference yield:

: 110-89-4
piperidine

: 2739-97-1
pyridine-2-acetonitrile

: 78-84-2
isobutyraldehyde

: 22346-07-2
4-methyl-2-(2-pirydyl)-2-pentenenitrile

Guidance literature:: With acetic acid; In benzene;

Reference yield:

: 109-04-6
2-bromo-pyridine

: 78-84-2
isobutyraldehyde

: 7605-28-9
2-(phenylsulfonyl)acetonitrile

: 22346-07-2
4-methyl-2-(2-pirydyl)-2-pentenenitrile

Guidance literature:: With sodium hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Yield given. Multistep reaction; 1.) DME; 2.) DMF, 15 h;
DOI:10.1248/cpb.38.1513