2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester
• CAS No.: 37275-47-1
• Deprecated CAS: 115713-95-6,124187-68-4,131649-62-2,132902-90-0,124187-68-4,131649-62-2,132902-90-0
• Molecular Formula: C12H18 O5
• Molecular Weight: 242.272
• Hs Code.: 2916190090
• European Community (EC) Number: 253-435-5
• DSSTox Substance ID: DTXSID0068024
• Nikkaji Number: J25.507F
• Wikidata: Q81994720
• Mol file: 37275-47-1.mol

Synonyms:37275-47-1;Trimethylolpropane diacrylate;2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester;2-Ethyl-2-(hydroxymethyl)-1,3-propanediyl diacrylate;EINECS 253-435-5;1,1,1-tris(hydroxymethyl)propane diacrylate;2-Propenoic acid, 1,1'-(2-ethyl-2-(hydroxymethyl)-1,3-propanediyl) ester;[2-(hydroxymethyl)-2-(prop-2-enoyloxymethyl)butyl] prop-2-enoate;trimethylol-propane diacrylate;SCHEMBL9577936;DTXSID0068024;2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediylester

Chemical Property of 2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester

Chemical Property:

• Vapor Pressure: 1.37E-06mmHg at 25°C
• Boiling Point: 358.7°Cat760mmHg
• Flash Point: 130.3°C
• PSA: 72.83000
• Density: 1.094g/cm³
• LogP: 0.83350
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 10
• Exact Mass: 242.11542367
• Heavy Atom Count: 17
• Complexity: 271

Purity/Quality:

99.0% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(CO)(COC(=O)C=C)COC(=O)C=C

Technology Process of 2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester

There total 3 articles about 2-Propenoic acid, 2-ethyl-2-(hydroxymethyl)-1,3-propanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.1%

1,1,1-tri(hydroxymethyl)propane (77-99-6) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → trimethylolpropyl tri(methyl)acrylate + trimethylolpropane diacrylate (37275-47-1)

Guidance literature:

With potassium carbonate; 4-methoxy-phenol; Reflux;

Reference yield:

trans-3-phenylprop-2-enyl chloride (21087-29-6) + 1,1,1-tri(hydroxymethyl)propane (77-99-6) + 4-methoxy-phenol (150-76-5) + acrylic acid (79-10-7) → trimethylolpropane diacrylate (37275-47-1)

Guidance literature:

In Petroleum ether;

Reference yield:

→ trimethylolpropane diacrylate (37275-47-1)

Guidance literature:

upstream raw materials:

trans-3-phenylprop-2-enyl chloride

1,1,1-tri(hydroxymethyl)propane

4-methoxy-phenol

acrylic acid

Downstream raw materials:

2-((acryloyloxy)methyl)-2-ethylpropane-1,3-diyl diacrylate

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